Cool Stuff > Crystallization K - 12 and Other Stuff > Growing Inorganic Crystals
Growing Inorganic Crystals  
For those students requesting recipes for growing inorganic crystals, here ya go. Be sure to have parental supervision and follow the safety precautions appropriate for the reagents used in the experiment.

Growing a crystal garden

You will need:
1. A plastic container, like a large margarine tub
2. Pieces of charcoal, pieces of broken clay flowerpots, and bits of sponge
3. Salt
4. Liquid laundry bluing*
5. Household ammonia (Ammonia is an irritant. That means it will stink your nose off. Keep it away from your face.)
5. A plastic cup
6. A tablespoon
7. Water

Day One:
Put the charcoal and the fragments of pot and sponge into the butter tub. Soak these parts in water for 15 minutes, then drain. Sprinkle over the fragments:
2 tablespoon of water
2 tablespoons of salt
2 tablespoons of bluing

This tub full will look pretty terrible at the beginning.

Day Two:
Sprinkle on two more tablespoons of salt. It will still look terrible today.

Day Three:
In the plastic cup, mix together 2 tablespoons of salt, 2 tablespoons of water, 2 tablespoons of bluing, and 2 tablespoons of ammonia. Stir well and carefully pour the solution into the bottom of the container - not on the crystals. It still will look and smell like a horrible blue glop, but then it begins to change....

Now what happens???
When your crystals stop growing, mix up another batch of solution like you did for day number three, and spoon it onto the materials. New crystals will form. You may also try adding some drops of food coloring or watercolors to your garden.

*liquid laundry bluing may be hard to find at your grocery store. You can write Mrs. Stewart's Liquid Bluing at Luther Ford & Co, P.O. Box 201405, Bloomington, MN 55420. They also have directions for a science project showing crystal growth.

Potassium aluminum sulfate dodecahydrate

Colorless. Cubic system.
KAl(SO4)2·12H2O

Make the following supersaturated solution:

1 a. 4 ounces of alum in 567 milliliters (19 ounces) of water
or
b. 20 grams per 100 milliliters of water

Add to the saturated solution:

2 a. 22 grams alum
or
b. 4 grams alum per original 100 milliliters of water

If the crystals grow too quickly they will have many veils and appear milky. To prevent this, reduce the amount of alum added in step 2.

Reference:
Crystals and crystal growing. Alan Holden and Phylis Morrison, The MIT Press, 1982, ISBN 0-262-58050-0

Borax

Na2B4O7·7H2O

Add one teaspoon of borax to 4 ounces of very hot water.
Stir until borax is completely dissolved. When this solutions cools to room temperature little borax crystals will grow.

Reference:
Crystals - A Handbook For School Teachers by Elizabeth A. Wood 1972. Written for the Commission on Crystallographic Teaching of the International Union of Crystallography.

To obtain a copy of this book contact the Polycrystal Book Service (Telephone & Fax: (513) 223-9070).

Alum

NH4Al(SO4)2·12H2O

Add 4 teaspoons of alum powder to four ounces of hot water.
Stir until alum is completely dissolved. Place a paper towel over the top of the jar containing the solution and secure with a rubber band. This will prevent dust from entering the solution but allow for evaporation.
After a period of time, given adequate evaporation, alum crystals will appear.

Reference:
Crystals - A Handbook For School Teachers by Elizabeth A. Wood 1972. Written for the Commission on Crystallographic Teaching of the International Union of Crystallography.

To obtain a copy of this book contact the Polycrystal Book Service (Telephone & Fax: (513) 223-9070).

Epsom Salt

MgSO4·7H2O

Add 6 teaspoons of epsom salt to 2 ounces of hot water.
Stir until epsom salt is completely dissolved. If all the salt does not dissolve, add a very small amount of water and stir until all the epsom salt is dissolved.
Place a paper towel over the top of the jar containing the solution and secure with a rubber band. This will prevent dust from entering the solution but allow for evaporation. After a period of time, given adequate evaporation, epsom salt crystals will appear.

Reference:
Crystals - A Handbook For School Teachers by Elizabeth A. Wood 1972. Written for the Commission on Crystallographic Teaching of the International Union of Crystallography.

To obtain a copy of this book contact the Polycrystal Book Service (Telephone & Fax: (513) 223-9070).
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